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Conductometric determination of ammonium ion with a mobile drop
Talanta 132:884 (2015)A mobile drop based approach was utilized for the conductometric determination of aqueous ammonium ion. A liquid drop was manipulated by gravity to remain or move out of a conductivity measurement zone located on a hydrophobic path. A dilute sulfuric acid drop functioned as a micro gas abs...
Fluorophotometric determination of critical micelle concentration (CMC) of ionic and non-ionic surfactants with carbon dots via Stokes shift
Talanta 132:572 (2015)A new and facile method for the determination of critical micelle concentration (CMC) of ionic and non-ionic surfactants is proposed in this article. Carbon dots exhibited substantial fluorescence and therefore enhanced the sensitivity of this evaluation. Understanding the formation of sur...
Direct electrodeposition of cable-like CuO@Cu nanowires array for non-enzymatic sensing
Talanta 132:719 (2015)Vertically aligned cable-like CuO@Cu nanowires array was synthesized using a template-directed electrodeposition strategy. The morphology, crystal structure, and surface property of nanowires array were investigated by SEM, HRTEM, XRD, and XPS, respectively. It is found that the free stand...
Determination of pesticide residues in samples of green minor crops by gas chromatography and ultra performance liquid chromatography couple...
Talanta 132:197 (2015)A method was developed for pesticide analysis in samples of high chlorophyll content belonging to the group of minor crops. A new type of sorbent, known as ChloroFiltr, was employed for dispersive-solid phase extraction cleanup (dispersive-SPE) to reduce the unwanted matrix background prio...
Electrochemical detection of ractopamine at arrays of micro-liquid | liquid interfaces
Talanta 132:205 (2015)The behaviour of protonated ractopamine (RacH+) at an array of micro-interfaces between two immiscible electrolyte solutions (micro-ITIES) was investigated via cyclic voltammetry (CV) and linear sweep stripping voltammetry (LSSV). The micro-ITIES array was formed at silicon membranes conta...
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Talanta 124:IFC (2014)
Design of molecularly imprinted polymers for diphenylamine sensing.
A series of the polymers imprinted with diphenylamine (DPA) and respective non imprinted polymers were synthesized using precipitation polymerization. Synthesized polymers were characterized by Fourier Transform Infra-Red spectroscopy with Total Attenuated Reflectance (FTIR-ATR), Sca...
Halogen-free ionic liquid as an additive in zinc(II)-selective electrode: surface analyses as correlated to the membrane activity.
Two conventional Zn(II) polyvinyl chloride (PVC) membrane electrodes have been prepared and characterized. They were based on dibenzo-24-crown-8 (DBC) as a neutral carrier, dioctyl phthalate (DOP) as a plasticizer, and potassium tetrakis (p-chlorophenyl) borate, KTpClPB or the haloge...
Optimization of horseradish peroxidase-catalyzed enhanced chemiluminescence reaction by full factorial design.
Using a full factorial design the optimization of experimental conditions of enhanced chemiluminescence reaction (ECR) catalyzed by horseradish peroxidase (HRP-C) in the presence of 3-(10'-phenothiazinyl)propane-1-sulfonate (SPTZ) and 4-morpholinopyridine (MORP) as enhancers was perf...
Metabonomic study on the cumulative cardiotoxicity of a pirarubicin liposome powder.
Our results confirm that when encapsulated into liposomes, the cumulative cardiotoxicity of THP can be greatly ameliorated. Lipophilic aglycone metabolites of THP associated with redox cycling are cardiotoxic for the possibility of reactive oxygen species (ROS) formation. Also, metabonomic analysis...