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Determination of deoxynivalenol and nivalenol by liquid chromatography and fluorimetric detection with on-line chemical post-column derivati...
A rapid, sensitive and selective analytical method was developed for the quantitative determination of deoxynivalenol (DON) and nivalenol (NIV) in cereals intended for human and animal consumption. The method, based on liquid chromatography and fluorescence detection, involves an aut...
A simple way to configure on-line two-dimensional liquid chromatography for complex sample analysis: acquisition of four-dimensional data.
An on-line comprehensive two-dimensional liquid chromatography (HPLC×UPLC-TOF MS) was set up just using the injection valve of the ultra performance liquid chromatography (UPLC) as the interface through which the effluent of high performance liquid chromatography (HPLC) was injected...
Use of flat-sheet membrane extraction with a sorbent interface for solvent-free determination of BTEX in water.
An analytical method for solvent-free determination of benzene, toluene, ethylbenzene, and xylenes (BTEX) in water using flat-sheet membrane extraction with a sorbent interface (MESI) coupled to GC-MS was established by optimizing the flow rates of the donor (20ml water) and acceptor...
A novel reverse phase stability indicating RP-UPLC method for the quantitative determination of fifteen related substances in Ranolazine dru...
A gradient reverse-phase ultra performance liquid chromatographic (RP-UPLC) method was developed for the quantitative determination of Ranolazine and potential process-related impurities (starting materials, positional isomers, degradants and byproducts) at the level of 0.1μgmL(-1)...
Seventeenth International Conference on Flow Injection Analysis.
Simultaneous determination of vanadium(IV) and vanadium(V) by flow injection analysis using kinetic spectrophotometry with Xylenol Orange.
A flow injection method of analysis has been developed for the simultaneous determination of V(IV) and V(V) using the difference in the rate of complex formation between vanadium in two different oxidation states and Xylenol Orange in acidic media. The proposed method used a spectrop...
Evaluation of acetylcysteine promoting effect on CdTe nanocrystals photoluminescence by using a multipumping flow system.
A simple and straightforward quantification method integrated in a fully automated multi-pumping flow system (MPFS) using water-soluble mercaptopropionic acid (MPA)-capped CdTe quantum dots (QDs) was implemented for the fluorescence quantification of N-acetyl-l-cysteine (NAC) in phar...
Towards the development of a miniaturized fiberless optofluidic biosensor for glucose.
A miniaturized fiberless optical sensor integrated in an automated sequential injection (SI) manifold for mesofluidic handling of sample, conditioning and regeneration solutions is herein proposed for monitoring glucose (as a model analyte) in human serum. The optofluidic biosensor c...
Flow injection determination of hydrogen peroxide using catalytic effect of cobalt(II) ion on a dye formation reaction.
A novel flow injection photometric method was developed for the determination of hydrogen peroxide in rainwater. This method is based on a cobalt(II)-catalyzed oxidative coupling of 3-methyl-2-benzothiazolinone hydrazone (MBTH) with N-ethyl-N-(2-hydroxy-3-sulfopropyl)-3,5-dimethoxyan...
A non-extractive sequential injection method for determination of molybdenum.
A non-extractive sequential injection spectrophotometric method for the determination of molybdenum has been developed. The method is based on the reaction between the thiocyanate complex of molybdenum and the polymethine dye (2-[2-(4-dipropylamino-phenyl)-vinyl]-1,3,3-trimethyl-3H-i...