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Non-enzymatic glucose sensors based on controllable nanoporous gold/copper oxide nanohybrids
Talanta 125:366 (2014)A kind of dealloyed nanoporous gold (NPG)/ultrathin CuO film nanohybrid for non-enzymatic glucose sensing has been prepared by a simple, in-situ, time-saving and controllable two-step electrodeposition. The three-dimensional and bicontinuous nanoporous structure of the nanocomposites have...
Reliable quantification of bisphenol A and its chlorinated derivatives in human urine using UPLC–MS/MS method
Talanta 125:284 (2014)We have comprehensively validated a method using salting-out assisted liquid/liquid extraction (SALLE) coupled to UPLC–MS/MS and isotope dilution quantification, to measure unconjugated BPA and ClxBPA in human urine according to the accepted guidelines. Deutered BPA as well as deutered 2,2′-DCBPA wa...
Design of molecularly imprinted polymers for diphenylamine sensing.
A series of the polymers imprinted with diphenylamine (DPA) and respective non imprinted polymers were synthesized using precipitation polymerization. Synthesized polymers were characterized by Fourier Transform Infra-Red spectroscopy with Total Attenuated Reflectance (FTIR-ATR), Sca...
Halogen-free ionic liquid as an additive in zinc(II)-selective electrode: surface analyses as correlated to the membrane activity.
Two conventional Zn(II) polyvinyl chloride (PVC) membrane electrodes have been prepared and characterized. They were based on dibenzo-24-crown-8 (DBC) as a neutral carrier, dioctyl phthalate (DOP) as a plasticizer, and potassium tetrakis (p-chlorophenyl) borate, KTpClPB or the haloge...
Optimization of horseradish peroxidase-catalyzed enhanced chemiluminescence reaction by full factorial design.
Using a full factorial design the optimization of experimental conditions of enhanced chemiluminescence reaction (ECR) catalyzed by horseradish peroxidase (HRP-C) in the presence of 3-(10'-phenothiazinyl)propane-1-sulfonate (SPTZ) and 4-morpholinopyridine (MORP) as enhancers was perf...
Metabonomic study on the cumulative cardiotoxicity of a pirarubicin liposome powder.
Our results confirm that when encapsulated into liposomes, the cumulative cardiotoxicity of THP can be greatly ameliorated. Lipophilic aglycone metabolites of THP associated with redox cycling are cardiotoxic for the possibility of reactive oxygen species (ROS) formation. Also, metabonomic analysis...
Determination of maleic hydrazide residues in garlic bulbs by HPLC.
In recent years, the release of information about the preventative and curative properties of garlic on different diseases and their benefits to human health has led to an increase in the consumption of garlic. To meet the requirements of international markets and reach competitivene...
Facile synthesis of N-acetyl-l-cysteine capped ZnS quantum dots as an eco-friendly fluorescence sensor for Hg^2^+
Trace analysis of acidic pharmaceutical residues in waters with isotope dilution gas chromatography-mass spectrometry via methylation deriva...
Using second-order calibration method based on trilinear decomposition algorithms coupled with high performance liquid chromatography with d...